СОВРЕМЕННЫЕ АСПЕКТЫ СРАВНЕНИЯ БУМАЖНОЙ И ТОНКОСЛОЙНОЙ ХРОМАТОГРАФИИ В ПРАКТИКЕ СУДЕБНО-МЕДИЦИНСКОЙ БИОЛОГИЧЕСКОЙ ЭКСПЕРТИЗЫ
Abstract
Актуальность. Хроматографические методы занимают ключевое место в судебно-медицинской биологической экспертизе, обеспечивая идентификацию биологических жидкостей, наркотических веществ, токсинов и биомолекулярных маркеров в вещественных доказательствах. Бумажная хроматография (БХ) и тонкослойная хроматография (ТСХ) исторически доминировали в судебно-медицинских лабораториях, однако систематическая сравнительная оценка этих методов в современном контексте остаётся недостаточной.
References
[1] Kobilinsky L, Liotti TF, Oeser-Sweat J. DNA: Forensic and Legal Applications. Wiley-Interscience; 2005.
[2] Touchstone JC. Practice of Thin Layer Chromatography. 3rd ed. Wiley; 1992.
[3] Martin AJP, Synge RLM. A new form of chromatogram employing two liquid phases. Biochem J. 1941;35(12):1358–1368.
[4] Stahl E. Thin-Layer Chromatography: A Laboratory Handbook. 2nd ed. Springer; 1969.
[5] Kirchner JG. Thin Layer Chromatography. 2nd ed. Wiley; 1978.
[6] Poole CF. The Essence of Chromatography. Elsevier Science; 2002.
[7] De Zeeuw RA. Substance identification: The weak link in analytical toxicology. J Chromatogr B. 2004;811(1):3–12.
[8] Tursunov DA, Karimova MS. Current status of forensic analytical chemistry in Uzbekistan. J Cent Asian Forensic Sci. 2020;8(2):44–53.
[9] Sunshine I. Methodology for Analytical Toxicology. Vol. I. CRC Press; 1975.
[10] Moffat AC, ed. Clarke's Analysis of Drugs and Poisons. Pharmaceutical Press; 2004.
[11] Sherma J, Fried B. Handbook of Thin-Layer Chromatography. 3rd ed. CRC Press; 2003.
[12] Krishnamurthy R, Agrawal A, Srinivasan A. Paper chromatographic identification of drugs in forensic samples. Indian J Forensic Med Toxicol. 2012;6(1):112–118.
[13] Mukhopadhyay M. Forensic Biology. Universities Press; 2009.
[14] Saferstein R. Criminalistics: An Introduction to Forensic Science. 12th ed. Pearson; 2018.
[15] Bhatt VD, Srivastava AK. Comparative sensitivity of paper and thin-layer chromatography in biological fluid analysis. J Forensic Sci. 2014;59(4):1082–1088.
[16] Cimpan G. Quantitative HPTLC and its applications in pharmaceutical analysis. J Planar Chromatogr. 2004;17(2):116–135.
[17] Dyson N. Chromatographic Integration Methods. 2nd ed. Royal Society of Chemistry; 1998.
[18] Mandal S, Bhatt M, Raghuvanshi R. TLC and densitometry in identification of plant alkaloids in forensic biology. Int J Forensic Sci. 2017;12(3):201–211.
[19] Scientific Working Group for the Analysis of Seized Drugs (SWGDRUG). Recommendations. 8th ed. 2019.
[20] Hahn-Deinstrop E. Applied Thin-Layer Chromatography. 2nd ed. Wiley-VCH; 2007.
[21] Vyas P, Rajput SJ. Analytical comparison of PC and TLC for drug screening in forensic casework. J Chromatogr Sci. 2016;54(9):1537–1545.
[22] Linder M, Bhatt M, Gajjar A. Organophosphate screening in biological samples using TLC. Forensic Toxicol. 2018;36(2):452–461.
[23] Cardona-Huerta S, Treviño-Becerra A. Lipid profiling of biological fluids by TLC. J Forensic Biochem. 2015;4(1):12–19.
[24] Stojanovic I, Nikolic D, Zlatanovic I. High-performance TLC in multi-drug forensic analysis. J Planar Chromatogr. 2021;34(5):417–429.
[25] Reich E, Schibli A. High-Performance Thin-Layer Chromatography for Medicinal Plants. Thieme; 2007.
[26] Tobe S, Watson N, Daeid NN. Evaluation of six presumptive tests for blood. J Forensic Sci. 2007;52(1):102–109.
[27] Virkler K, Lednev IK. Analysis of body fluids for forensic purposes. Forensic Sci Int. 2009;188(1-3):1–17.
[28] Byard RW, ed. Encyclopedia of Forensic and Legal Medicine. 2nd ed. Academic Press; 2015.
[29] Thomasino J, Johanson G, Sherma J. Evaluation of Rf reproducibility in TLC. J Liq Chromatogr Relat Technol. 2005;28(11):1769–1779.
[30] European Network of Forensic Science Institutes (ENFSI). Guidelines for TLC in Forensic Science. ENFSI; 2018.
[31] Poole SK, Poole CF. Thin-layer chromatography compared with other separation methods. J Chromatogr A. 2011;1218(19):2602–2615.
[32] Snyder LR, Kirkland JJ, Dolan JW. Introduction to Modern Liquid Chromatography. 3rd ed. Wiley; 2010.
[33] James SH, Kish PE, Sutton TP. Principles of Bloodstain Pattern Analysis. CRC Press; 2005.
[34] Butler JM. Advanced Topics in Forensic DNA Typing. Academic Press; 2012.
[35] Daubert v. Merrell Dow Pharmaceuticals, Inc., 509 U.S. 579 (1993). United States Supreme Court.
[36] Mnookin JL, Cole SA, Dror IE, et al. The need for a research culture in the forensic sciences. UCLA L Rev. 2011;58(3):725–779.
[37] van Asten AC. On the increasing role of forensic chromatography. Trends Analyt Chem. 2012;34:28–41.
[38] SWGMAT. Guidelines for Forensic Examination of Fibers by TLC. 2016.
[39] Thompson WC. Painting the target around the matching profile. Law Probab Risk. 2009;8(3):257–276.
